Page 58 - 5010
P. 58

25 ml, four test tubes of capacity 10 ml and eight test tubes of capacity
                  5 ml. The frequency of rotor rotation from  2000 to 8000 revolutions/
                  minute is regulated by steps. The separation factor reaches up to 6000.
                  The time of rotor acceleration to the maximum frequency of rotation

                  is  8  –  10 minutes.  The  centrifuge  is  equipped  by electric  watch.  Its
                  using  makes  possible  to  set  the  time  of  centrifugation  from  0  to
                  60 minutes  with  the  following  automatic  braking.  The mass  of

                  the centrifuge is 16 kg).
                        In  the  centrifuge,  at very proof  emulsions, decomposition  does
                  not go to the end and instead  of  water the  enriched emulsion with
                  less quantity of water is  got  and  besides all mechanical admixtures,

                  so-called “mud”, are separated.
                        This method of demulsification is  not  used in  the  fields in large
                  scales because of  high cost of  centrifuges.

                        The content of water and mud in oil samples is determined, as a
                  rule, by means of small centrifuges in field laboratories.
                        The    most  commonly  used    are    centrifuges    with    the    drive

                  from    an    electric    motor    with   rotation    frequency   approximately
                  3000 revolutions/minute and more.
                        Figure 8.1 shows the centrifuge with test tubes.

                        During  the  work with centrifuges with the  electric drive  it  is
                  forbidden:
                  - to work without earthing;
                  - to   increase   the  rotation  frequency over  the  maximum  magnitude

                  (for   the  centrifuge  of   LTC-2  (ЦЛН–2)  type  this  magnitude  is
                  8000 revolutions/minute);
                  - to work with the open covers of rotor and centrifuge;

                  -  to work with glass test  tubes at rotation  frequency more  than  1/2  of
                  the maximum magnitude (for the centrifuge of  LTC-2 (ЦЛН–2) type
                  this magnitude is 4000 revolutions/minute);
                  - to  place  not  diametrically  opposite  the  test  tubes  filled  with

                  centrifugal material (centrifugate).
                        Besides the centrifuges mentioned above such modern centrifuges
                  are produced by industry:

                         1) The  portable   laboratory   centrifuge  ОПн-3.02  (the
                  centrifuge    of    periodical    type    with   frequency of   rotation   up  to
                  3000  revolutions/minute  (fig. 8.2). It  is  used   for   separation  of

                  the  heterogeneous  liquid  systems  into  fractions  (for liquids  with


                                                              57
   53   54   55   56   57   58   59   60   61   62   63