Page 45 - 5010
P. 45

6.4.2 Determining the density of liquid (formation water)
                                              by means of pycnometer.

                        6.4.2.1 Determine the mass of  dried  and cooled to the ambient

                  temperature empty pycnometer with accuracy 0.0002 g (m, g).
                        6.4.2.2 Pour  the  distilled  water  into pycnometer by means of
                  the funnel a little bit over the mark (for pycnometers of the 2nd, 3rd

                  and 5th types) and to the top (for pycnometer of the 4th type).
                        Сlose pycnometer by plug and put it into the water thermostat for
                  20 minutes (keep the constant temperature of water in the thermostat
                  20 °С ± 0,1 °С).


                        6.4.2.3  Take    pycnometer  out   of   the  thermostat,  wipe  it,  fix


                  accurately the level of water in it to the mark by means of the filter
                  paper and determine the mass of pycnometer with distilled water (with

                  the accuracy 0.0002 g) – m , g.
                                                     1

                        6.4.2.4 Discharge pycnometer, wipe and dry it and pour the tested

                  liquid (for example, formation water) into pycnometer  (accurately to
                  the mark). And then repeat the same operations with the tested liquid
                  (formation  water)  and  as  the  result  you  will  get  the  mass  of

                  pycnometer  with  the  tested liquid (m , g).


                                                                   2

                        6.4.2.5 The density of  the  tested  liquid  by means of pycnometer

                  is calculated  by the following equation:


                                                      (m  -  m) 0.99823
                                               ρ    l  20    2          ,                              (6.6)
                                                           m   -  m
                                                             1

                  where  ρ  is the density of  the tested  liquid determined by means of
                               l  20
                                                                                  3
                  pycnometer  under  the  temperature  20  °С,  g/сm ;  m  is  the  mass  of
                  dried  empty  pycnometer,  g;  m is  the  mass  of    pycnometer  with

                                                            1
                  distilled  water,  g;  m is  the  mass  of pycnometer  with  the  tested
                                               2

                  liquid (for example formation water), g; 0.99823 is the magnitude of
                                                                                                3
                  density  of  distilled water under the temperature 20 °С, g/сm .
                        6.4.2.6  Put  the  results   of  the  measurements   by  means  of

                  pycnometer into table 6.4.
                        6.4.2.7 Draw the conclusion.



                                                              44
   40   41   42   43   44   45   46   47   48   49   50